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Shuh, David

TitleChemist Sr Staff Sci/Engr
InstitutionLawrence Berkeley National Lab
DepartmentChemical Sciences
Address1 Cyclotron Road
Berkeley CA 94720
Phone510/486-6937
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    Collapse Research 
    Collapse Research Activities and Funding
    Biomimetic Actinide Decorporation: Characterization and Preclinical Development
    NIH/NIAID RC2AI087604Sep 28, 2009 - Aug 31, 2012
    Role: Co-Principal Investigator

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    Publications listed below are automatically derived from MEDLINE/PubMed and other sources, which might result in incorrect or missing publications. Researchers can login to make corrections and additions, or contact us for help.
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    1. Altman AB, Brown AC, Rao G, Lohrey TD, Britt RD, Maron L, Minasian SG, Shuh D, Arnold J. Chemical structure and bonding in a thorium(iii)-aluminum heterobimetallic complex. Chem Sci. 2018 May 14; 9(18):4317-4324. PMID: 29780563.
      View in: PubMed
    2. Pacold JI, Altman AB, Knight KB, Holliday KS, Kristo MJ, Minasian SG, Tyliszczak T, Booth CH, Shuh D. Development of small particle speciation for nuclear forensics by soft X-ray scanning transmission spectromicroscopy. Analyst. 2018 Mar 12; 143(6):1349-1357. PMID: 29479614.
      View in: PubMed
    3. Minasian SG, Batista ER, Booth CH, Clark DL, Keith JM, Kozimor SA, Lukens WW, Martin RL, Shuh D, Stieber SCE, Tylisczcak T, Wen XD. Quantitative Evidence for Lanthanide-Oxygen Orbital Mixing in CeO2, PrO2, and TbO2. J Am Chem Soc. 2017 Dec 13; 139(49):18052-18064. PMID: 29182343.
      View in: PubMed
    4. Yeung CT, Yim KH, Wong HY, Pal R, Lo WS, Yan SC, Yee-Man Wong M, Yufit D, Smiles DE, McCormick LJ, Teat SJ, Shuh D, Wong WT, Law GL. Chiral transcription in self-assembled tetrahedral Eu4L6 chiral cages displaying sizable circularly polarized luminescence. Nat Commun. 2017 Oct 24; 8(1):1128. PMID: 29066720.
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    5. Altman AB, Pemmaraju CD, Alayoglu S, Arnold J, Booth CH, Braun A, Bunker CE, Herve A, Minasian SG, Prendergast D, Shuh D, Tyliszczak T. Chemical and Morphological Inhomogeneity of Aluminum Metal and Oxides from Soft X-ray Spectromicroscopy. Inorg Chem. 2017 May 15; 56(10):5710-5719. PMID: 28471186.
      View in: PubMed
    6. Dalodière E, Virot M, Morosini V, Chave T, Dumas T, Hennig C, Wiss T, Dieste Blanco O, Shuh D, Tyliszcak T, Venault L, Moisy P, Nikitenko SI. Insights into the sonochemical synthesis and properties of salt-free intrinsic plutonium colloids. Sci Rep. 2017 Mar 03; 7:43514. PMID: 28256635.
      View in: PubMed
    7. Lukens WW, Magnani N, Tyliszczak T, Pearce CI, Shuh D. Incorporation of Technetium into Spinel Ferrites. Environ Sci Technol. 2016 Dec 06; 50(23):13160-13168. PMID: 27934274.
      View in: PubMed
    8. Cross JN, Macor JA, Bertke JA, Ferrier MG, Girolami GS, Kozimor SA, Maassen JR, Scott BL, Shuh D, Stein BW, Stieber SC. Comparing the 2,2'-Biphenylenedithiophosphinate Binding of Americium with Neodymium and Europium. Angew Chem Int Ed Engl. 2016 Oct 04; 55(41):12755-9. PMID: 27629989.
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    9. Maloubier M, Shuh D, Minasian SG, Pacold JI, Solari PL, Michel H, Oberhaensli FR, Bottein Y, Monfort M, Moulin C, Den Auwer C. How Do Radionuclides Accumulate in Marine Organisms? A Case Study of Europium with Aplysina cavernicola. Environ Sci Technol. 2016 Oct 04; 50(19):10730-10738. PMID: 27588898.
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    10. Dau PD, Shuh D, Sturzbecher-Hoehne M, Abergel RJ, Gibson JK. Divalent and trivalent gas-phase coordination complexes of californium: evaluating the stability of Cf(ii). Dalton Trans. 2016 Aug 02; 45(31):12338-45. PMID: 27424652.
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    11. Butorin SM, Kvashnina KO, Vegelius JR, Meyer D, Shuh D. High-resolution X-ray absorption spectroscopy as a probe of crystal-field and covalency effects in actinide compounds. Proc Natl Acad Sci U S A. 2016 07 19; 113(29):8093-7. PMID: 27370799; PMCID: PMC4961124 [Available on 01/19/17].
    12. Demir S, Brune NK, Van Humbeck JF, Mason JA, Plakhova TV, Wang S, Tian G, Minasian SG, Tyliszczak T, Yaita T, Kobayashi T, Kalmykov SN, Shiwaku H, Shuh D, Long JR. Extraction of Lanthanide and Actinide Ions from Aqueous Mixtures Using a Carboxylic Acid-Functionalized Porous Aromatic Framework. ACS Cent Sci. 2016 Apr 27; 2(4):253-65. PMID: 27163056; PMCID: PMC4850516.
    13. Butorin SM, Modin A, Vegelius JR, Suzuki MT, Oppeneer PM, Andersson DA, Shuh D. Local Symmetry Effects in Actinide 4f X-ray Absorption in Oxides. Anal Chem. 2016 Apr 19; 88(8):4169-73. PMID: 27008406.
      View in: PubMed
    14. Xian L, Tian G, Beavers CM, Teat SJ, Shuh D. Glutarimidedioxime: A Complexing and Reducing Reagent for Plutonium Recovery from Spent Nuclear Fuel Reprocessing. Angew Chem Int Ed Engl. 2016 Apr 04; 55(15):4671-3. PMID: 26970221.
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    15. Dumas T, Guillaumont D, Fillaux C, Scheinost A, Moisy P, Petit S, Shuh D, Tyliszczak T, Den Auwer C. The nature of chemical bonding in actinide and lanthanide ferrocyanides determined by X-ray absorption spectroscopy and density functional theory. Phys Chem Chem Phys. 2016 Jan 28; 18(4):2887-95. PMID: 26733312.
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    16. Tian G, Shuh D, Beavers CM, Teat SJ. A structural and spectrophotometric study on the complexation of Am(III) with TMOGA in comparison with the extracted complex of DMDOOGA. Dalton Trans. 2015 Nov 14; 44(42):18469-74. PMID: 26442451.
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    17. Altman AB, Pemmaraju CD, Camp C, Arnold J, Minasian SG, Prendergast D, Shuh D, Tyliszczak T. Theory and X-ray Absorption Spectroscopy for Aluminum Coordination Complexes – Al K-Edge Studies of Charge and Bonding in (BDI)Al, (BDI)AlR2, and (BDI)AlX2 Complexes. J Am Chem Soc. 2015 Aug 19; 137(32):10304-16. PMID: 26258886.
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    18. Löble MW, Keith JM, Altman AB, Stieber SC, Batista ER, Boland KS, Conradson SD, Clark DL, Lezama Pacheco J, Kozimor SA, Martin RL, Minasian SG, Olson AC, Scott BL, Shuh D, Tyliszczak T, Wilkerson MP, Zehnder RA. Covalency in lanthanides. An X-ray absorption spectroscopy and density functional theory study of LnCl6(x-) (x = 3, 2). J Am Chem Soc. 2015 Feb 25; 137(7):2506-23. PMID: 25689484.
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    19. Gianetti TL, Nocton G, Minasian SG, Kaltsoyannis N, Kilcoyne ALD, Kozimor SA, Shuh D, Tyliszczak T, Bergman RG, Arnold J. Electron localization in a mixed-valence diniobium benzene complex. Chem Sci. 2015 Feb 01; 6(2):993-1003. PMID: 29560186.
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    20. Liu M, Wang J, Wu X, Wang E, Abergel RJ, Shuh D, Raymond KN, Liu P. Characterization, HPLC method development and impurity identification for 3,4,3-LI(1,2-HOPO), a potent actinide chelator for radionuclide decorporation. J Pharm Biomed Anal. 2015 Jan; 102:443-9. PMID: 25459944; PMCID: PMC4314361.
    21. Tian G, Shuh D. A spectrophotometric study of Am(III) complexation with nitrate in aqueous solution at elevated temperatures. Dalton Trans. 2014 Oct 21; 43(39):14565-9. PMID: 24999760.
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    22. Pemmaraju CD, Copping R, Wang S, Janousch M, Teat SJ, Tyliszcak T, Canning A, Shuh D, Prendergast D. Bonding and charge transfer in nitrogen-donor uranyl complexes: insights from NEXAFS spectra. Inorg Chem. 2014 Nov 03; 53(21):11415-25. PMID: 25330350.
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    23. Ward MD, Mesbah A, Minasian SG, Shuh D, Tyliszczak T, Lee M, Choi ES, Lebègue S, Ibers JA. Synthesis and characterization of eight compounds of the MU8Q17 family: ScU8S17, CoU8S17, NiU8S17, TiU8Se17, VU8Se17, CrU8Se17, CoU8Se17, and NiU8Se17. Inorg Chem. 2014 Jul 07; 53(13):6920-7. PMID: 24932673.
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    24. Meihaus KR, Minasian SG, Lukens WW, Kozimor SA, Shuh D, Tyliszczak T, Long JR. Influence of pyrazolate vs N-heterocyclic carbene ligands on the slow magnetic relaxation of homoleptic trischelate lanthanide(III) and uranium(III) complexes. J Am Chem Soc. 2014 Apr 23; 136(16):6056-68. PMID: 24650296.
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    25. Copping R, Jeon B, Pemmaraju CD, Wang S, Teat SJ, Janousch M, Tyliszczak T, Canning A, Grønbech-Jensen N, Prendergast D, Shuh D. Toward equatorial planarity about uranyl: synthesis and structure of tridentate nitrogen-donor {UO2}2+ complexes. Inorg Chem. 2014 Mar 03; 53(5):2506-15. PMID: 24528285.
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    26. Butorin SM, Shuh D, Kvashnina KO, Guo J, Werme L, Nordgren J. Chemical reduction of actinides probed by resonant inelastic X-ray scattering. Anal Chem. 2013 Dec 03; 85(23):11196-200. PMID: 24187957.
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    27. Minasian SG, Keith JM, Batista ER, Boland KS, Kozimor SA, Martin RL, Shuh D, Tyliszczak T, Vernon LJ. Carbon K-edge X-ray absorption spectroscopy and time-dependent density functional theory examination of metal-carbon bonding in metallocene dichlorides. J Am Chem Soc. 2013 Oct 02; 135(39):14731-40. PMID: 24047199.
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    28. La Pierre HS, Minasian SG, Abubekerov M, Kozimor SA, Shuh D, Tyliszczak T, Arnold J, Bergman RG, Toste FD. Vanadium bisimide bonding investigated by X-ray crystallography, 51V and 13C nuclear magnetic resonance spectroscopy, and V L(3,2)-edge X-ray absorption near-edge structure spectroscopy. Inorg Chem. 2013 Oct 07; 52(19):11650-60. PMID: 24024833.
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    29. Gianetti TL, Nocton G, Minasian SG, Tomson NC, Kilcoyne AL, Kozimor SA, Shuh D, Tyliszczak T, Bergman RG, Arnold J. Diniobium inverted sandwich complexes with µ-?6:?6-arene ligands: synthesis, kinetics of formation, and electronic structure. J Am Chem Soc. 2013 Feb 27; 135(8):3224-36. PMID: 23343247.
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    30. Minasian SG, Keith JM, Batista ER, Boland KS, Bradley JA, Daly SR, Kozimor SA, Lukens WW, Martin RL, Nordlund D, Seidler GT, Shuh D, Sokaras D, Tyliszczak T, Wagner GL, Weng TC, Yang P. Covalency in metal-oxygen multiple bonds evaluated using oxygen K-edge spectroscopy and electronic structure theory. J Am Chem Soc. 2013 Feb 06; 135(5):1864-71. PMID: 23351138.
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    31. Spencer LP, Yang P, Minasian SG, Jilek RE, Batista ER, Boland KS, Boncella JM, Conradson SD, Clark DL, Hayton TW, Kozimor SA, Martin RL, MacInnes MM, Olson AC, Scott BL, Shuh D, Wilkerson MP. Tetrahalide complexes of the [U(NR)2]2+ ion: synthesis, theory, and chlorine K-edge X-ray absorption spectroscopy. J Am Chem Soc. 2013 Feb 13; 135(6):2279-90. PMID: 23320417.
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    32. Law GL, Andolina CM, Xu J, Luu V, Rutkowski PX, Muller G, Shuh D, Gibson JK, Raymond KN. Circularly polarized luminescence of curium: a new characterization of the 5f actinide complexes. J Am Chem Soc. 2012 Sep 19; 134(37):15545-9. PMID: 22920726; PMCID: PMC3477521.
    33. Yang Y, Saiers JE, Xu N, Minasian SG, Tyliszczak T, Kozimor SA, Shuh D, Barnett MO. Impact of natural organic matter on uranium transport through saturated geologic materials: from molecular to column scale. Environ Sci Technol. 2012 Jun 05; 46(11):5931-8. PMID: 22533547.
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    34. Minasian SG, Boland KS, Feller RK, Gaunt AJ, Kozimor SA, May I, Reilly SD, Scott BL, Shuh D. Synthesis and structure of (Ph4P)2MCl6 (M = Ti, Zr, Hf, Th, U, Np, Pu). Inorg Chem. 2012 May 21; 51(10):5728-36. PMID: 22554112.
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    35. Minasian SG, Keith JM, Batista ER, Boland KS, Clark DL, Conradson SD, Kozimor SA, Martin RL, Schwarz DE, Shuh D, Wagner GL, Wilkerson MP, Wolfsberg LE, Yang P. Determining relative f and d orbital contributions to M-Cl covalency in MCl6(2-) (M = Ti, Zr, Hf, U) and UOCl5(-) using Cl K-edge X-ray absorption spectroscopy and time-dependent density functional theory. J Am Chem Soc. 2012 Mar 28; 134(12):5586-97. PMID: 22404133.
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    36. Rios D, Rutkowski PX, Shuh D, Bray TH, Gibson JK, Van Stipdonk MJ. Electron transfer dissociation of dipositive uranyl and plutonyl coordination complexes. J Mass Spectrom. 2011 Dec; 46(12):1247-54. PMID: 22223415.
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    37. Sturzbecher-Hoehne M, Leung CN, D'Aléo A, Kullgren B, Prigent AL, Shuh D, Raymond KN, Abergel RJ. 3,4,3-LI(1,2-HOPO): in vitro formation of highly stable lanthanide complexes translates into efficacious in vivo europium decorporation. Dalton Trans. 2011 Sep 07; 40(33):8340-6. PMID: 21766096.
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    38. Bugaris DE, Choi ES, Copping R, Glans PA, Minasian SG, Tyliszczak T, Kozimor SA, Shuh D, Ibers JA. Pentavalent and tetravalent uranium selenides, Tl3Cu4USe6 and Tl2Ag2USe4: syntheses, characterization, and structural comparison to other layered actinide chalcogenide compounds. Inorg Chem. 2011 Jul 18; 50(14):6656-66. PMID: 21678928.
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    39. Ni C, Shuh D, Raymond KN. Uranyl sequestration: synthesis and structural characterization of uranyl complexes with a tetradentate methylterephthalamide ligand. Chem Commun (Camb). 2011 Jun 14; 47(22):6392-4. PMID: 21552620.
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    40. Dähn R, Vespa M, Tyliszczak T, Wieland E, Shuh D. Soft X-ray spectromicroscopy of cobalt uptake by cement. Environ Sci Technol. 2011 Mar 01; 45(5):2021-7. PMID: 21265566.
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    41. Bradley JA, Yang P, Batista ER, Boland KS, Burns CJ, Clark DL, Conradson SD, Kozimor SA, Martin RL, Seidler GT, Scott BL, Shuh D, Tyliszczak T, Wilkerson MP, Wolfsberg LE. Experimental and theoretical comparison of the O K-edge nonresonant inelastic X-ray scattering and X-ray absorption spectra of NaReO4. J Am Chem Soc. 2010 Oct 06; 132(39):13914-21. PMID: 20839792.
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    42. Fillaux C, Guillaumont D, Berthet JC, Copping R, Shuh D, Tyliszczak T, Den Auwer C. Investigating the electronic structure and bonding in uranyl compounds by combining NEXAFS spectroscopy and quantum chemistry. Phys Chem Chem Phys. 2010 Nov 14; 12(42):14253-62. PMID: 20886130.
      View in: PubMed
    43. Abergel RJ, Durbin PW, Kullgren B, Ebbe SN, Xu J, Chang PY, Bunin DI, Blakely EA, Bjornstad KA, Rosen CJ, Shuh D, Raymond KN. Biomimetic actinide chelators: an update on the preclinical development of the orally active hydroxypyridonate decorporation agents 3,4,3-LI(1,2-HOPO) and 5-LIO(Me-3,2-HOPO). Health Phys. 2010 Sep; 99(3):401-7. PMID: 20699704; PMCID: PMC2921233.
    44. Bugaris DE, Copping R, Tyliszczak T, Shuh D, Ibers JA. La2U2Se9: an ordered lanthanide/actinide chalcogenide with a novel structure type. Inorg Chem. 2010 Mar 01; 49(5):2568-75. PMID: 20136071.
      View in: PubMed
    45. Abergel RJ, D'Aléo A, Leung CN, Shuh D, Raymond KN. Using the antenna effect as a spectroscopic tool: photophysics and solution thermodynamics of the model luminescent hydroxypyridonate complex [Eu(III)(3,4,3-LI(1,2-HOPO))]-. Inorg Chem. 2009 Dec 07; 48(23):10868-70. PMID: 19902920; PMCID: PMC2873866.
    46. Minasian SG, Krinsky JL, Rinehart JD, Copping R, Tyliszczak T, Janousch M, Shuh D, Arnold J. A comparison of 4f vs 5f metal-metal bonds in (CpSiMe3)3M-ECp* (M = Nd, U; E = Al, Ga; Cp* = C5Me5): synthesis, thermodynamics, magnetism, and electronic structure. J Am Chem Soc. 2009 Sep 30; 131(38):13767-83. PMID: 19725526.
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    47. Abergel RJ, Clifton MC, Pizarro JC, Warner JA, Shuh D, Strong RK, Raymond KN. The siderocalin/enterobactin interaction: a link between mammalian immunity and bacterial iron transport. J Am Chem Soc. 2008 Aug 27; 130(34):11524-34. PMID: 18680288; PMCID: PMC3188318.
    48. Gorden AE, Xu J, Szigethy G, Oliver A, Shuh D, Raymond KN. Characterization of a mixed salt of 1-hydroxypyridin-2-one Pu(IV) complexes1. J Am Chem Soc. 2007 May 30; 129(21):6674-5. PMID: 17488009.
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    49. McKeown DA, Buechele AC, Lukens WW, Shuh D, Pegg IL. Tc and Re behavior in borosilicate waste glass vapor hydration tests. Environ Sci Technol. 2007 Jan 15; 41(2):431-6. PMID: 17310703.
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    50. Abergel RJ, Warner JA, Shuh D, Raymond KN. Enterobactin protonation and iron release: structural characterization of the salicylate coordination shift in ferric enterobactin. J Am Chem Soc. 2006 Jul 12; 128(27):8920-31. PMID: 16819888; PMCID: PMC3188320.
    51. Nilsson HJ, Tyliszczak T, Wilson RE, Werme L, Shuh D. Soft X-ray scanning transmission X-ray microscopy (STXM) of actinide particles. Anal Bioanal Chem. 2005 Sep; 383(1):41-7. PMID: 16021423.
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    52. Lukens WW, Bucher JI, Shuh D, Edelstein NM. Evolution of technetium speciation in reducing grout. Environ Sci Technol. 2005 Oct 15; 39(20):8064-70. PMID: 16295876.
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    53. Gorden AE, Shuh D, Tiedemann BE, Wilson RE, Xu J, Raymond KN. Sequestered plutonium: [Pu(IV){5LIO(Me-3,2-HOPO)}2]--the first structurally characterized plutonium hydroxypyridonate complex. Chemistry. 2005 Apr 22; 11(9):2842-8. PMID: 15744705.
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    54. Nachimuthu P, Thevuthasan S, Adams EM, Weber WJ, Begg BD, Mun BS, Shuh D, Lindle DW, Gullikson EM, Perera RC. Near-edge X-ray absorption fine structure study of disordering in Gd2(Ti1-yZry)2O7 pyrochlores. J Phys Chem B. 2005 Feb 03; 109(4):1337-9. PMID: 16851100.
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    55. Yoon TH, Johnson SB, Benzerara K, Doyle CS, Tyliszczak T, Shuh D, Brown GE. In situ characterization of aluminum-containing mineral-microorganism aqueous suspensions using scanning transmission X-ray microscopy. Langmuir. 2004 Nov 23; 20(24):10361-6. PMID: 15544358.
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    56. Lukens WW, Shuh D, Schroeder NC, Ashley KR. Identification of the non-pertechnetate species in Hanford waste tanks, Tc(I)--carbonyl complexes. Environ Sci Technol. 2004 Jan 01; 38(1):229-33. PMID: 14740740.
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    57. Lukens WW, Bucher JI, Edelstein NM, Shuh D. Products of pertechnetate radiolysis in highly alkaline solution: structure of TcO2 x xH2O. Environ Sci Technol. 2002 Mar 01; 36(5):1124-9. PMID: 11918000.
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